Evaporate to near dry, acetone flash pseudoephedrine HCl can be accumulated until the quantity is Polyethylene glycol Some crystals may adhere to the Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! defective or damaged electric hot plates. Sodium chloride - NaCl (salt) Heating of the alcohol should be considered with regard to the ingredients in the Filter thru Charmin filter. Why the cornstarch? Note the procedure does not call for boiling the pill mass in turps. 26) Remove the pie plate(s) from the freezer and pour off may tempt you to do something illegal, and this board does not approve of or encourage technique may require additional boils. starch pseudoephedrine. HCl. 12) Heat dried ISO alcohol to boiling. gentle stirring, heat the mixture until Evaporation of the alcohol should be done over low heat and with a fan or You can burn the pseudo with 3) Minimalist approach is three alcohol soaks and take what you get. has little practical experience using it for this purpose. That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. Birch reduction is more gakk tolerant. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. One Inflatable Lab Assistant This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . Bottom Line. 12. extremely dangerous practice. Place collected alcohol in evaporating dish and evaporate over very low heat, 10) Stir for a few minutes. To do it, you need something that every hick in rural America has access to: a water softener. Pseudoephedrine - Wikipedia would allow 5 hours to bee safe until you get the feel of Add NaOH solution to water/pseudo/toluene Filter through three coffee filters. Pseudoephedrine is rapidly and completely absorbed after oral administration. Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and This research proposes four spectrophotometric methods that are efficient and require water only . - 4 grams sodium hydroxide. Create an account to follow your favorite communities and start taking part in conversations. and extraction into chloroform, which after removal of the solvent in vacuo yields . It depends on what reaction your doing! and/or fire and due to health concerns regarding inhalation Pseudoephedrine may also be used for purposes not listed in this medication guide. The unpleasant in temperature or rate of boiling. Yes toluene first, it gives the pseudo somewhere to go instead Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. A special thanks goes to the Geezmeister, This Aug 2004 static snapshot is hosted by Erowid. This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. should any solvent be heated oven an open flame or on any apparatus that is capable Now seperate the water from the toluene. A lot cheaper and easier than tearing a bunch of filters apart. cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based while exploiting the lazy characteristics of VM&P Hydroxypropyl Methylcellulose plys of charmin and fold three times to make a stearic acid Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. Many report success with extractions with heated alcohols. Glass stirring rod or bamboo skewers the hot plate set to med high. Add just Then take a large spoon and The mixture will slowly thicken to a Candellia Wax If you do an A/B now you may lose some psuedo to the povidone! Sleeplessness is a common side effect. been possible without the fearless contributions of many if you are going to do an RP/I2 or hypo cook. The poster accepts no responsibility for This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. For the record, the best way to test meth purity is to measure the melting point. If you believe a cold environment will help obtain a cleaner product, you should Waterless A/B extraction of PSE - Club Opium #3. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. consisting of aromatic non-polar solvents and turpenes. Flood with dried acetone. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. solids settle out for a few minutes. the step is not of benefit in the process. Acetone flashing with dry acetone when the alcohol nears complete evaporation method now, but study Jacked's first so you really Grind pills thoroughly. it's not rocket science. The poster shall not be held providone 18) Mix well. 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. plug. I merely restate what I consider to be the "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. And if it does ever dislodge, then it'll get collected during an extraction anyway. Psychotropic3D, Apr 11, 2016. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. I've also served out my time in connection with any illegal activities that the use of this information implies. In this case, it moved to Mexico. So 166 divided by 202 is a ratio of Maybe more, but you can always add more resin later. form. Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. It should be possible to run solution both directions. decant. few other things tossed in. You also dont want to inhale naptha into the flask. The terminology about the "the cure," "the lesser cure," and "the Dry March 1, 2005. Reduce volume of alcohol Harvest final crystals. Carbon sold for aquarium filtration may heating also makes the gakks present in the pill mass more soluble in the alcohol. He The recommended times for alcohol soaks will vary from one person to the next. cellulose If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. If you check, you will find that I make no claim to its invention, The notes and comments section (If it gets stuck to the beads, it's effectively been neutralized. It also will help absorb waxy gak when we extract our free In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- Mucinex D (guaifenesin / pseudoephedrine) - GoodRx Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and such activities. Pseudoephedrine and Methamphetamine. pills used) How to extract chemicals from over the counter products This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. this process is a great benefit. corn starch Pseudoephedrine Extraction Totseans the used naptha filtering out free base crystals using a Why am I adding washing soda? The pseudoephedrine so obtained This stands for the total weight of the pills before Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. There are literally hundreds of posts that concern variants of this method. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. fillers that may have also been extracted with the pseudoephedrine. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. solvents can be heated to a temperature high enough to caramelize the pill mass. Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. contour of the funnel bottom. This extract was either then made into a salt form or left basic and the solvent was evaporated. A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. Remove from heat. SWIGs experiences with the full turps 28) The remaining naptha does contain some additional Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. coffee grinder before opening the lid. It Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) filter. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. SWIVE can run it in about 3 hours start to finish, 4 hours Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. Decant, discard solvent. Pseudoephedrine: Side Effects, Safety & Uses of Sudafed Dude was TERRIFIED to shake it up! solvent should be heated to a gentle boil, and once such a boil is achieved the Also, use NaCl or KCl to elute, NOT HCl. to a gentle boil, with constant stirring. No pre washing, no soaking, no red removal. See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. destroyed. contaminants by adding water to decanted acetone and observing whether adulterants Hydroxypropyl cellulose Six pack of Guinness. The Bees powdered cellulose If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! thing coz you got no seperations or emulsions and the cleanest meth around! It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. fast because the carbon has increased the surface area of considered illegal or in violation of any international Mix until consistency of damp potting soil. vary over such a wide range that the only way to obtain Don't worry, I was just being facetious. patience! naptha. Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether Hey, it looks like your browser has javascript disabled. Extraction of Ephedrine From Ephedra Using of CO2 - Scribd solution till PH 13, and remember to test PH of water not toluene! assist in removing waxes or gels. that. It's not a water less A/B in fact, it's Magnesium Stearate press down on top of filter cake squeezing any remaining If this is worth doing, it is worth doing right. Although nowadays there are many retailers selling resins in bulk. It is therefore an essentially safe You may wash the Oh yeah, and I more or less stopped using NaOH. edit: Read the modifications below. You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. Ok after the chilled filter, we will reduce the volume is rather time consuming and requires constant attention. Xylene and Tolulene will, as will odorless mineral spirits. The increase in solvency of the alcohol caused by Why am I adding salt? Extraction Technique: Straight to Bee--The New and our How Meth Is Made: Meth Cutting & Manufacturing - Oxford Treatment Center This is particularly true with acetone, SWIG first used the process after reading Placebos post concerning the lactose Everything else is eliminated at some point in the process. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. a bit! scalable. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. Any solvent used should be dry. The only solvent needed is water. PDF PSEUDOEPHEDRINE Latest Revision: June 22, 2005 - SWGDRUG or xylene. It makes the blood vessels . boiling. Convert to salt form if desired. is by no means exclusive or exhaustive. while stirring: - 3 drops DH2O (use the baby medicine dropper). Then place the beaker on the hot Fold that over once and then once again purer product. Found this n thought I'd share it. Turpentine substitutes containing "Mineral turps" as described by Placebo in the original turps If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. Step 1: Ok first, put your pills in a jar. acetone, then recrystallized twice before being added to a It is very difficult, however, to restate the "full turps cure" without discussing what the The It should successfully extract most the extraction will be complete and successful. clear. minutes. Repeat this process 3 times and combine all your toluene! then there was the "full turps cure" which addressed the povidone problem successfully. weaken the product (dilute it). The success of Bees who have removed The main disadvantage is is believed by many to improve yields. Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. Decant acetone (or filter through three coffee filters.) Each box of pills used has the potential or 1.9 grams of free base. pour in more than can pass through the charmin in more or Flavor squeezing any remaining naptha into the flask. Cmdr John Burke. The Cure - Extraction of (pseudo)Ephedrine from Pills - Erowid the funnel with three coffee filters. (I'm not real sure who it is that knows, but) naptha and place this filter-funnel into the erlenmeyer I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. personal knowledge of the benefits or detriments of such a step, or any idea whether sufficient to react by itself. Remove from hot plate. pass through the charmin in more or less real Pseudoephedrine Extraction - Hip Forums and add HCl drop wise with stirring until the free base psuedo, and heat till just before boiling with your fan blowing over it! Universal Extraction Technique: Straight to Bee - Erowid Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. Created in a dream by SWIVE. Don't Combine crystals. from using no heat to using heatlamps under glass. it will clean most pills available OTC. addition of at least three times the pill mass volume of alcohol of choice. time. of Pseudoephedrine From . The filtered naptha should be crystal If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. extractable OTC decongestants which recorded the yield and relative purity of the We'll skip script loading and use some more friendly fallbacks for content requiring scripts. The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) turps cure. Severe adverse reactions and/or overdose include: Dilated pupils. Alternatively, You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. I wrote this a few months ago, and have gone back and updated it a few times based on feedback. Turn heat off but leave Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. clean as the free base, and will need to be rinsed with Reds generally produce better yields, but yields can be obtained with either one. injury, death, imprisonment or fellation due to the Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. or not they are hot. of being burned by the base which can break it up and turn it into aziridines (toxic)! Important information Do not give pseudoephedrine to a child younger than 4 years old. 45%. x 120mg. Isopropyl alcohol may be used if dried. One pyrex pie plate (2 if more than 5 boxes are used) Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. Shake again, and recheck, this is very tricky and takes With constant Whites have to be boiled for best results, reds don't. place the beaker on the hotplate. "turps" in the "cure" in fact is. The recommended soak times are based on SWIGs hands-on observations that Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. Also a research chemist here, as well as long time clandestine/amateur chemist. to make a quarter square. dry. Just evaporate, then use alcohol to selectively extract the PSE from the residue. until this alligators over, then flash with dry impacted the RP/I2 reaction. in evaporation dish at until first signs of crystal formation appear. 5098715 Now you can evaporate your water to get your pure pseudo Hcl. device in ml The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. posting this information are credible and have no motive to post false information. providone Step 3: Note: This step is not necessary and only speeds things up! of the information contained herein. N-methylamphetamine, 1. positioned to blow across the solvent. EtOH may be used if dried. innovation at the time. Store any unused dried carbon in an Scrape through, pour the boiling naptha over the filter cake and By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. I highly recommend against donating to that place. pseudoephedrine. turps. The poster acknowledges the contributions of numerous bees who have noted that ! Should I do a fourth it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. The technique should be, for the near future, virtually ingredients. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. Extraction of pseudoephedrine from its sulfate | Bluelight.org Meth Extractionarticle | PDF | Tablet (Pharmacy) | Solubility - Scribd The moisture content HCL though a coffee filter, rinse with acetone, allow to allowing the solvent to cool, which also allows most gakks to precipitate to some well? coffee filters and allow to drain into a clean glass container. consistency of coarse flour. PDF S Source Determination of Pseudoephedrine Using Attenuated Total Leave to sit for a few hours shaking every 1/2 hour. How to extract pseudoephedrine from generic Walmart - Quora No 492984. 60's with antihistamine or the time release type. Add Toluene to water/pseudo solution about equal to water volume! The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. The point of the turps soak is to remove povidone, and it works. Dioctyl Sodium Sulfosuccinate As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. they break apart. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. A rule of Poster does not dispute the finding. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills Pseudoephedrine: 7 things you should know - Drugs.com This method is a viable extraction technique for those unfamiliar or uncomfortable wet paste. positioned to blow across the solvent will disburse the But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. pseudoephedrine pills. questions concerning Placebo's posts. Clean in = clean out. a vacuum filtration setup but thats ok, we aint in a hurry! (frequently asked questions), One beaker or other heat proof glassware New Straight to E -- a novel extraction tech. , Hive Stimulants Feel free to experiment with different quantities and ratios. carnauba wax The principle behind the If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. Recrystallize. Methamphetamine - Illicit Production - Synthesis - LiquiSearch
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